Synthesis of thienylhydrogermanes and their transformations in the presence of di(<i>tert</i>-butyl) peroxide

Authors

  • Э. Лукевиц Latvian Institute of Organic Synthesis, Riga LV-1006
  • O. A. Пудова Latvian Institute of Organic Synthesis, Riga LV-1006
  • И. Мажейка Latvian Institute of Organic Synthesis, Riga LV-1006
  • C. Гринбеpга Latvian Institute of Organic Synthesis, Riga LV-1006

Abstract

A method was developed for the synthesis of thienylhydrogermanes RnGeH4−n (where R=2-thienyl, n=1–3), involving the reduction of the corresponding ethoxygermanes by lithium aluminum hydride under the conditions of phase-transfer catalysis. The transformations of thienylhydrogermanes under the influence of di(tert-butyl) peroxide were studied. Features of the mass-spectrometric behavior of thienylethoxygermanes were analyzed.

How to Cite
Lukevics, E.; Pudova, O. A.; Mazheika, I.; Grinbergs, S. Chem. Heterocycl. Compd. 1997, 33, 171. [Khim. Geterotsikl. Soedin. 1997, 198.]

For this article in the English edition, see DOI https://doi.org/10.1007/BF02256758

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Published

1997-02-25

Issue

No. 2 (1997)

Section

Original Papers