COPPER-CATALYZED ARYLATION OF TETRAZOLE-5-THIONES UPON CONVECTION HEATING AND MICROWAVE ACTIVATION CONDITIONS
DOI:
https://doi.org/10.1007/1262Keywords:
aryl iodide, cuprous chloride, ethylenediamine, tetrazole-5-thione, arylation, microwave activationAbstract
The arylation of 1-phenyltetrazole-5-thione using a series of iodobenzene derivatives in the presence of cuprous chloride and a ligand such as ethylenediamine. It was shown that the use of microwave activation permitted shortening of the reaction time, increasing yields and simplification of the reaction products isolation.
Authors: U. N. Dmitrieva, S. M. Ramsh, Yu. E. Zevatskii, T. V. Artamonova, and L. V. Myznikov.
English translation in Chemistry of Heterocyclic Compounds, 2012, 48 (2), pp 355-357
http://link.springer.com/article/10.1007/s10593-012-0996-0