REGULARITIES AND FEATURES OF THE REACTION OF 2-AMINO-6-NITRO- AND 2,6-DIAMINOBENZOTHIAZOLES WITH ETHYLENE CHLOROHYDRIN

Authors

  • P. Ф. Амбарцумова S. Yunusov Institute of the Chemistry of Plant Substances, Academy of Sciences of the Republic of Uzbekistan, Tashkent 700170
  • Б. Ташходжаев S. Yunusov Institute of the Chemistry of Plant Substances, Academy of Sciences of the Republic of Uzbekistan, Tashkent 700170
  • M. Ю. Антипин A. N. Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, Moscow 119991
  • Х. M. Шахидоятов S. Yunusov Institute of the Chemistry of Plant Substances, Academy of Sciences of the Republic of Uzbekistan, Tashkent 700170

Keywords:

2-aminobenzothiazoles, benzothiazoline-2-thiones, 2-iminobenzothiazoles, ethylene chlorohydrin, hydroxyalkylation, X-ray analysis

Abstract

The alkylation of 2-amino-6-nitro- and 2,6-diaminobenzothiazoles by ethylene chlorohydrin has been studied. A comparative analysis has been made of the composition of these reaction mixtures and of those obtained from other 2-aminobenzothiazoles using this reaction. The structure of the synthesized compounds was confirmed using IR and 1H NMR spectroscopy, mass spectrometry, and X-ray diffraction and via alternative syntheses.

How to Cite
Ambartsumova, R. F.; Tashkhodzhaev, B.; Antipin, M. Yu.; Shakhidoyatov,Kh. M. Chem. Heterocycl. Compd. 2002, 38, 1397. [Khim. Geterotsikl. Soedin. 2002, 1582.]

For this article in the English edition, see DOI https://doi.org/10.1023/A:1022194829594

Published

2002-11-25

Issue

Section

Original Papers