NEW METHOD OF SYNTHESIS OF 5-ACETYL-3-CYANO-6-METHYLPYRIDINE-2(1H)-THIONE AND ITS PROPERTIES

Authors

  • Я. Ю. Якунин Lugansk Taras Shevchenko State Pedagogical University, Lugansk 91011
  • B. Д. Дяченко Lugansk Taras Shevchenko State Pedagogical University, Lugansk 91011
  • В. П. Литвинов N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, Moscow 117913

Keywords:

5-acetyl-3-cyano-6-methylpyridine-2(1H)-thione, alkylation

Abstract

5-Acetyl-3-cyano-6-methylpyridine-2(1H)-thione was obtained by the reaction of ethoxymethyleneacetylacetone with cyanothioacetamide in the presence of N-methylmorpholine. Its alkylation, bromination of the 2-methylthio derivative, and the conversions of its 5-bromoacetyl derivative have been studied.

How to Cite
Yakunin, Ya. Yu.; Dyachenko, V. D.; Litvinov, V. P. Chem. Heterocycl. Compd. 2001, 37, 581. [Khim. Geterotsikl. Soedin. 2001, 633.]

For this article in the English edition, see DOI https://doi.org/10.1023/A:1011656605605

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Published

2001-05-25

Issue

No. 5 (2001)

Section

Original Papers