SILICA-SUPPORTED SODIUM HYDROGEN SULFATE CATALYZED SYNTHESIS OF 13-ARYL-12<i>H</i>-DIBENZO[<i>b</i>,<i>i</i>]XANTHENE-5,7,12,14(13<i>H</i>)-TETRAONES

Authors

  • D. Liu Shandong University of Science and Technology
  • J. Gao Shandong University of Science and Technology
  • L. Li Shandong University of Science and Technology
  • S. Zhou Shandong University of Science and Technology
  • D. Xu Shandong University of Science and Technology

DOI:

https://doi.org/10.1007/982

Keywords:

aldehyde, dibenzo[b, i]xanthenes, 2-hydroxy-1, 4-naphthoquinone, silica-supported sodium hydrogen sulfate, solvent-free reaction

Abstract

13-Aryl-12H-dibenzo[b,i]xanthene-5,7,12,14(13H)-tetraone derivatives were synthesized by the one-pot condensation of 2-hydroxy-1,4-naphthoquinone and aldehydes under solvent-free conditions with good yields in the presence of silica-supported sodium hydrogen sulfate as heterogeneous catalyst. The catalyst is easily prepared, reusable, low-cost, and environment-friendly under the reaction conditions.

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Published

2013-09-26

Issue

No. 9 (2013)

Section

Original Papers