SYNTHESIS OF THE FIRST DITHIAAZA-17-CROWN-5 ETHERS CONTAINING PIPERIDIN-4-ONE SUBUNIT

Authors

  • Thanh Van Tran Thi Faculty of Chemistry, VNU University of Science, Vietnam National University, Hanoi, 334 Nguyen Trai St., Thanh Xuan, Hanoi 100000, Vietnam
  • Manh Linh Nguyen Faculty of Chemistry, VNU University of Science, Vietnam National University, Hanoi, 334 Nguyen Trai St., Thanh Xuan, Hanoi 100000, Vietnam Faculty of Pharmacy, Thai Nguyen University of Medicine and Pharmacy, 284 Luong Ngoc Quyen St., Thai Nguyen City 250000, Vietnam
  • Tien Dat Nguyen Faculty of Chemistry, VNU University of Science, Vietnam National University, Hanoi, 334 Nguyen Trai St., Thanh Xuan, Hanoi 100000, Vietnam
  • The Duan Le Faculty of Chemistry, VNU University of Science, Vietnam National University, Hanoi, 334 Nguyen Trai St., Thanh Xuan, Hanoi 100000, Vietnam
  • Hong Hieu Truong Peoples’ Friendship University of Russia (RUDN University).
  • Victor N. Khrustalev RUDN University, 6 Miklukho-Maklaya St., Moscow 117198, Russia; e-mail: khrustalev-vn@rudn.ru N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, 47 Leninsky Ave., Moscow 119991, Russia; е-mail: vnkhrustalev@gmail.com
  • Tuan Anh Le Faculty of Chemistry, VNU University of Science, Vietnam National University, Hanoi, 334 Nguyen Trai St., Thanh Xuan, Hanoi 100000, Vietnam

DOI:

https://doi.org/10.1007/6277

Keywords:

dithiaaza-17-crown-5 ether, 2, 2'-[ethane-1, 2-diylbis(oxyethane-2, 1-diylsulfanediyl)]dibenzaldehyde, domino reaction, Petrenko– Kritschenko reaction.

Abstract

Dithiaaza-17-crown-5 ethers containing piperidin-4-one subunit and dithiacrown ether fragment were synthesized in one-pot Petrenko–Kritschenko reaction from 2,2'-[ethane-1,2-diylbis(oxyethane-2,1-diylsulfanediyl)]dibenzaldehyde, methyl ethyl ketone or dibenzyl ketone, and ammonium acetate. Molecular structure of dithiaaza-17-crown-5 ethers were confirmed by NMR, HRMS, and single crystal X-ray diffraction.

Author Biographies

Thanh Van Tran Thi, Faculty of Chemistry, VNU University of Science, Vietnam National University, Hanoi, 334 Nguyen Trai St., Thanh Xuan, Hanoi 100000, Vietnam

Assoc. Professor of Department of Organic Chemistry, Faculty of Chemistry.

Manh Linh Nguyen, Faculty of Chemistry, VNU University of Science, Vietnam National University, Hanoi, 334 Nguyen Trai St., Thanh Xuan, Hanoi 100000, Vietnam Faculty of Pharmacy, Thai Nguyen University of Medicine and Pharmacy, 284 Luong Ngoc Quyen St., Thai Nguyen City 250000, Vietnam

PhD student of Department of Organic Chemistry, Faculty of Chemistry, VNU-University of Science, Vietnam National University, Hanoi.

Tien Dat Nguyen, Faculty of Chemistry, VNU University of Science, Vietnam National University, Hanoi, 334 Nguyen Trai St., Thanh Xuan, Hanoi 100000, Vietnam

PhD student of Department of Organic Chemistry, Faculty of Chemistry.

The Duan Le, Faculty of Chemistry, VNU University of Science, Vietnam National University, Hanoi, 334 Nguyen Trai St., Thanh Xuan, Hanoi 100000, Vietnam

PhD of Faculty of Chemistry.

Hong Hieu Truong, Peoples’ Friendship University of Russia (RUDN University).

PhD of Faculty of Science, Peoples’ Friendship University of Russia (RUDN University)

Victor N. Khrustalev, RUDN University, 6 Miklukho-Maklaya St., Moscow 117198, Russia; e-mail: khrustalev-vn@rudn.ru N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, 47 Leninsky Ave., Moscow 119991, Russia; е-mail: vnkhrustalev@gmail.com

Professor of Faculty of Science, Peoples’ Friendship University of Russia (RUDN University)

Tuan Anh Le, Faculty of Chemistry, VNU University of Science, Vietnam National University, Hanoi, 334 Nguyen Trai St., Thanh Xuan, Hanoi 100000, Vietnam

Assoc. Professor of Department of Organic Chemistry, Faculty of Chemistry.

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Published

2021-10-21

Issue

Vol. 57 No. 10 (2021)

Section

Short Communications