Synthesis and crystalline and molecular structure of hydrochloride of 1-[2-(2,3-dihydro-1,3,4-oxadiazolyl-5-one)]methyl-7-bromo-5-phenyl-1,2-dihydro-3H-1,4-benzodiazepin-2-one

Authors

  • В. И. Павловский A. V. Bogatskii Physico-Chemical Institute, Ukraine Academy of Sciences, Odessa 270080
  • Ю. А. Симонов Institute of Applied Physics, Academy of Sciences of the Republic of Moldova, Kishinev 277028
  • А. А. Дворкин Institute of Applied Physics, Academy of Sciences of the Republic of Moldova, Kishinev 277028
  • А. C. Яворский A. V. Bogatskii Physico-Chemical Institute, Ukraine Academy of Sciences, Odessa 270080
  • М. Г. Рoкачинская A. V. Bogatskii Physico-Chemical Institute, Ukraine Academy of Sciences, Odessa 270080
  • C. А. Андронати A. V. Bogatskii Physico-Chemical Institute, Ukraine Academy of Sciences, Odessa 270080

Abstract

By the interaction of 1-hydrazinocarbonylinethyl-7-bromo-5-phenyl-1,2-dihydro-3H-1,4-benzodiazepin-2-one with phosgene, the compound 1-[2-(2,3-dihydro-1,3,4-oxadiazolyl-5-one)jmethyl-7-bromo-5-phenyl-1, 2-dihydro-3H-1,4-benzodiazepin-2-one has been synthesized. Spectroscopic methods and X-ray structure analysis have been used to establish the crystalline and molecular structure of this new derivative of 1,4-benzodiazepine.

How to Cite
Pavlovskii, V. I.; Simonov, Yu. A.; Dvorkin, A. A.; Yavorskii, A. S.; Rokachinskaya, M. G.; Andronati, S. A. Chem. Heterocycl. Compd. 1995, 31, 610. [Khim. Geterotsikl. Soedin. 1995, 689.]

For this article in the English edition, see DOI https://doi.org/10.1007/BF01166339

Published

1995-05-25

Issue

Section

Original Papers