7-BROMO-5-PHENYL-1,2-DIHYDRO-3H-1,3,5-BENZTRIAZEPIN-2-ONE

Authors

  • С. В. Власюк A. V. Bogatsky Institute of Physical Chemistry, Ukraine National Academy of Sciences, Odessa
  • В. И. Павловский A. V. Bogatsky Institute of Physical Chemistry, Ukraine National Academy of Sciences, Odessa
  • С. А. Андронати A. V. Bogatsky Institute of Physical Chemistry, Ukraine National Academy of Sciences, Odessa
  • М. Гданец Mickiewicz University, Faculty of Chemistry, Poznan
  • Ю. А. Симонов Institute of Applied Physics, Moldavian Academy of Sciences

DOI:

https://doi.org/10.1007/317

Keywords:

benztriazepine, semicarbazone of 2-aminobenzophenone, hydrogen bonds, IR spectroscopy, UV spectroscopy, X-ray crystallography

Abstract

7-Bromo-5-phenyl-1,2-dihydro-3H-1,4-benztriazepin-2-one was obtained by thermolysis of the syn-4-phenylsemicarbazone of 2-aminobenzophenone. It’s molecular and crystal structures were established by X ray crystallography. The nature of the hydrogen bonds between molecules of the compound in solution and in the crystalline state was determined by IR spectroscopy and X-ray crystallography.

Author: S. V. Vlasiuk, V. I. Pavlovsky, S. A. Andronati, M. Gdaniec, and Yu. A. Simonov.

English Translation in Chemistry of Heterocyclic Compounds, 2000, 36 (9), pp 1077-1085

http://link.springer.com/article/10.1023/A%3A1002790116884

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Published

2013-02-14

Issue

No. 9 (2000)

Section

Original Papers